Theory of dyeing of acid dye



Acid dye are easily applied on wool, silk and nylon fibres. During dyeing, H2SO4 or CH3-COOH is present due to perform dyed. They are water soluble and produce color anion and sodium cation.
RSO3Na ---------- RSO3- +Na+
Wool fibre polymer may be represent as:
H2N-W-COOH ------------- Wool
So there are present amino group of polymer part and other part contain carboxyl group.
Under certain condition, The hydrogen ion attached to the carboxyl group is transferred to the amino group at the other end of the macromolecule so that the two ends of the keratin molecular chain acquire opposite electrical charges:
H2N-W-COOH----------------H3N+-W-COO-
Thus when wool fibre is entered in a acid solution, negatively charged carboxylate group take up hydrogen ions released from hydrochloric acid group and the chloride anions, also released from HCl are absorbed by positively charged amino ends of the keratin macromolecule.
HCl ====H+ + Cl-
NH3+-W-COO- H+ Cl-  ========= ClNH3-W-COOH
When wool is immersed in acid solution, the concentration of acid is decreased by the absorption of acids with the formation of an electrically positive site whenever an amino group is present in the keratin molecule i.e. acids act as exhausting agents while dyeing acid dyes on wool. This absorption continues until equilibrium absorption and sodium chloride is formed as a result of forward reaction.Thus if the salt reaction is increased in the dye bath, the rate of backward reaction is increased. In fact act as a retarding agent in the dyeing of acid dyes on wool. In order to get uniform dyeing results the dyeing is started in the presence of salt with a small amount of an acid in the cold, followed by raising the temperature gradually. In order to exhaust the dye bath more of the acid is added to the dye bath and the dyeing aontinued..
Dyeing process sequence:
Dyeing
Washing
 
Neutralization
Soap wash & boiling